benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside
CAS No.:102794-20-7
Molecular Formula:C₃₉H₃₈Cl₆NO₁₃P
Molecular Weight:972.421
Hs Code.:

benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Synonyms:benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Chemical Property of benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Technology Process of benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

There total 5 articles about benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 102794-19-4
benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 102794-20-7
benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; In benzene; for 2h; Ambient temperature;
DOI:10.1248/cpb.33.4098

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 102794-20-7
benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetramethylurea / CH₂Cl₂ / 16 h / Ambient temperature

2: 87 percent / pyridine, 4-dimethylaminopyridine / benzene / 2 h / Ambient temperature

With pyridine; dmap; tetramethylurea; In dichloromethane; benzene;
DOI:10.1248/cpb.33.4098

Reference yield:

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 102794-20-7
benzyl 6-O-benzyloxymethyl-4-O-diphenylphosphono-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 4-dimethylaminopyridine / 2 h / Ambient temperature

2: 98 percent / 90percent acetic acid / H₂O / 0.25 h / 90 °C

3: 85 percent / tetramethylurea / CH₂Cl₂ / 16 h / Ambient temperature

4: 87 percent / pyridine, 4-dimethylaminopyridine / benzene / 2 h / Ambient temperature

With pyridine; dmap; acetic acid; tetramethylurea; In dichloromethane; water; benzene;
DOI:10.1248/cpb.33.4098