3,5-bisnitro-N,N-diprop-2-enylbenzamide

Base Information

• Chemical Name: 3,5-bisnitro-N,N-diprop-2-enylbenzamide
• CAS No.: 91768-82-0
• Molecular Formula: C₁₃H₁₃N₃O₅
• Molecular Weight: 291.263
• Mol file: 91768-82-0.mol

Synonyms:N,N-diallyl-3,5-dinitrobenzamide

Chemical Property of 3,5-bisnitro-N,N-diprop-2-enylbenzamide

Chemical Property:

• Boiling Point: 453.2±45.0 °C(Predicted)
• PKA: -3.24±0.70(Predicted)
• Density: 1.296±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-bisnitro-N,N-diprop-2-enylbenzamide

There total 2 articles about 3,5-bisnitro-N,N-diprop-2-enylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

diallylamine (124-02-7) + 3,5-dinitrobenoyl chloride (99-33-2) → N,N-diallyl-3,5-dinitrobenzamide (91768-82-0)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 24h; Sealed tube;

DOI:10.1021/jacs.5b00151

Reference yield:

→ N,N-diallyl-3,5-dinitrobenzamide (91768-82-0)

Guidance literature:

3.5-Dinitro-benzoylchlorid, Diallylamin in wss. NaHCO3;

Reference yield: 92.0%

N,N-diallyl-3,5-dinitrobenzamide (91768-82-0) → 1-(3,5-dinitrobenzoyl)-2,5-dihydro-1H-pyrrole

Guidance literature:

With Hoveyda-Grubbs catalyst second generation; sodium chloride; In ethyl acetate; for 3h; Reagent/catalyst; Milling;

DOI:10.1021/jacs.5b00151

upstream raw materials:

diallylamine

3,5-dinitrobenoyl chloride