N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

Base Information

Chemical Name:N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide
CAS No.:1335107-65-7
Molecular Formula:C₂₂H₃₆N₂O₆
Molecular Weight:424.538
Hs Code.:

Synonyms:N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

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Chemical Property of N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

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Technology Process of N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

There total 5 articles about N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1335107-57-7
8-(3,4-dihydro-8-isopentyl-2-oxo-2H-chromen-7-yloxy)octanoic acid

: 1335107-65-7
N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

Guidance literature:: 8-(3,4-dihydro-8-isopentyl-2-oxo-2H-chromen-7-yloxy)octanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 20 ℃; for 1h;

With hydroxylamine hydrochloride; potassium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.06.002

Reference yield:

: 8-isopentyl-7-hydroxy-chroman-2-one

: 1335107-65-7
N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium carbonate / acetone / 2 h / 56 °C / Inert atmosphere

2.1: methanol; lithium hydroxide / 2 h / 63 °C / Inert atmosphere

3.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1 h / 20 °C

3.2: 3 h / 20 °C

With methanol; 18-crown-6 ether; chloroformic acid ethyl ester; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; acetone;
DOI:10.1016/j.ejmech.2011.06.002

Reference yield:

: ethyl 8-(3,4-dihydro-8-isopentyl-2-oxo-2H-chromen-7-yloxy)octanoate

: 1335107-65-7
N-hydroxy-8-(3-hydroxy-4-(2-hydroxycarbamoylethyl)-2-isopentyl-phenoxy)octanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; lithium hydroxide / 2 h / 63 °C / Inert atmosphere

2.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1 h / 20 °C

2.2: 3 h / 20 °C

With methanol; chloroformic acid ethyl ester; triethylamine; lithium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2011.06.002