3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

Base Information

Chemical Name:3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide
CAS No.:1309364-97-3
Molecular Formula:C₂₄H₃₀N₄O
Molecular Weight:390.528
Hs Code.:

Synonyms:3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

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Chemical Property of 3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

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Technology Process of 3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

There total 6 articles about 3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309365-54-5
3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3dimethylbutyl)acrylamide

: 1309364-97-3
3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; for 4h;

Reference yield:

: 93493-66-4
N-(6-Chloro-4-formyl-3-pyridinyl)-2,2-dimethylpropanamide

: 1309364-97-3
3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium acetate / Pd catalyst / acetonitrile; water / 0.25 h / 100 °C / microwave irradiation

2.1: hydrogenchloride; water / 16 h / 100 °C

3.1: potassium carbonate / dimethyl sulfoxide / 2 h / 70 °C

4.1: sodium hydroxide; water / methanol / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / 1-methyl-pyrrolidin-2-one / 0.08 h

5.2: 1 h

6.1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h

With hydrogenchloride; water; hydrogen; potassium acetate; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1309365-53-4
3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)acrylic acid

: 1309364-97-3
3-(2-amino-6-o-tolyl-1,7-naphthyridin-3-yl)-N-(3,3-dimethylbutyl)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / 1-methyl-pyrrolidin-2-one / 0.08 h

1.2: 1 h

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h

With hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; ethanol;