S-benzyl phosphorodichloridothioate

Base Information

• Chemical Name: S-benzyl phosphorodichloridothioate
• CAS No.: 112994-25-9
• Molecular Formula: C₇H₇Cl₂OPS
• Molecular Weight: 241.078

Synonyms:S-benzyl phosphorodichloridothioate

Chemical Property of S-benzyl phosphorodichloridothioate

Chemical Property:

Purity/Quality:

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Technology Process of S-benzyl phosphorodichloridothioate

There total 3 articles about S-benzyl phosphorodichloridothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

dibenzyl disulphide (150-60-7) → S-benzyl phosphorodichloridothioate (112994-25-9)

Guidance literature:

With methyl dichlorophosphite; In liquid sulphur dioxide; at -68 ℃; for 0.5h;

DOI:10.1080/00397919208021305

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → S-benzyl phosphorodichloridothioate (112994-25-9)

Guidance literature:

With copper(I) chloride; magnesium chloride; trichlorophosphate; Heating; atmospheric pressure;

Reference yield:

→ S-benzyl phosphorodichloridothioate (112994-25-9)

Guidance literature:

PCl3, CH3-C(=O)-O-C(=O)-CH3, / CCl4, /BRN= 1110443/, SO2Cl2, Cl2, (-20-30grad);

upstream raw materials:

dibenzyl disulphide

benzyl alcohol

Downstream raw materials:

Trithiophosphoric acid S-benzyl ester S',S''-bis-(1-phenyl-ethyl) ester

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