Technology Process of ethyl 4-allyloxy-3-hydroxybutyrate
There total 1 articles about ethyl 4-allyloxy-3-hydroxybutyrate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: SnCl2 / CH2Cl2 / 0.25 h / 20 °C
1.2: 83 percent / CH2Cl2 / -10 - 20 °C
2.1: 80 percent / NaBH4 / ethanol / 0.17 h / -10 °C
With
sodium tetrahydroborate; tin(ll) chloride;
In
ethanol; dichloromethane;
DOI:10.1021/ol049493t
- Guidance literature:
-
With
calcium sulfate; silver(l) oxide;
In
benzene;
for 12h;
DOI:10.1021/ol049493t
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 97 percent / Ag2O; CaSO4 / benzene / 12 h
2: aq. LiOH / methanol / 3 h
3: Et3N / diethyl ether / 4 h / -10 °C
4: 200 mg / diethyl ether / 0 °C
5: 56 percent / Rh2(tpa)4 / hexane / 20 °C
With
calcium sulfate; lithium hydroxide; dirhodium(II) tetrakis(triphenylacetate); triethylamine; silver(l) oxide;
In
methanol; diethyl ether; hexane; benzene;
DOI:10.1021/ol049493t
