Chen-1-Bolm

Base Information

Chemical Name:Chen-1-Bolm
CAS No.:1383947-49-6
Molecular Formula:C₂₅H₂₇NOS
Molecular Weight:389.561
Hs Code.:

Synonyms:Chen-1-Bolm

Suppliers and Price of Chen-1-Bolm

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Chen-1-Bolm

Chemical Property:

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Technology Process of Chen-1-Bolm

There total 3 articles about Chen-1-Bolm which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1383947-45-2
PT# 1151456

: 1383947-49-6
Chen-1-Bolm

Guidance literature:: With sulfuric acid; In water; at 110 ℃; for 4h;
DOI:10.1016/j.bmcl.2012.05.018

Reference yield:

: 119-61-9
benzophenone

: 1383947-49-6
Chen-1-Bolm

Guidance literature:: Multi-step reaction with 4 steps

1: titanium tetrachloride; zinc / tetrahydrofuran; dichloromethane / 4.5 h / Reflux

2: [bis(acetoxy)iodo]benzene / acetonitrile / 1.5 h / 0 °C

3: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / methanol / 1.5 h / 0 - 20 °C

4: sulfuric acid / water / 4 h / 110 °C

With [bis(acetoxy)iodo]benzene; sulfuric acid; titanium tetrachloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 1: McMurry olefination;
DOI:10.1016/j.bmcl.2012.05.018

Reference yield:

: C₂₆H₂₆N₂S

: 1383947-49-6
Chen-1-Bolm

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / methanol / 1.5 h / 0 - 20 °C

2: sulfuric acid / water / 4 h / 110 °C

With sulfuric acid; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; water;
DOI:10.1016/j.bmcl.2012.05.018