Technology Process of 2,3,4-Trifluoropyridine
There total 1 articles about 2,3,4-Trifluoropyridine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium tetrafluorocobaltate(III);
In
gaseous matrix;
at 310 ℃;
for 3.5h;
Further byproducts given;
DOI:10.1016/S0022-1139(00)81239-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: i-Pr2NH; BuLi / tetrahydrofuran; hexane / 2 h / -75 °C
1.2: 82 percent / tetrahydrofuran; hexane / 1 h / -75 °C
2.1: 96 percent / hydrazine monohydrate / tetrahydrofuran / 20 h / 50 °C
3.1: 72 percent / tetrabutylammonium fluoride trihydrate / tetrahydrofuran / 2 h / 25 °C
4.1: 60 percent / MnO2 / octan-1-ol / 15 - 25 °C
With
manganese(IV) oxide; n-butyllithium; tetrabutyl ammonium fluoride; hydrazine hydrate; diisopropylamine;
In
tetrahydrofuran; octanol; hexane;
DOI:10.1002/chem.200400837
