3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

Base Information

Chemical Name:3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone
CAS No.:137351-35-0
Molecular Formula:C₁₉H₂₂O₃S₂
Molecular Weight:362.514
Hs Code.:

Synonyms:3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

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Chemical Property of 3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

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Technology Process of 3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

There total 2 articles about 3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 137351-39-4
1-Chloro-3,3-dimethyl-1-phenylsulfanyl-butan-2-one

: 824-79-3
sodium 4-methylbenzenesulfinate

: 137351-35-0
3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; In acetone; benzene; at 60 ℃; for 4h;
DOI:10.1080/00397919108019810

Reference yield:

: 37471-41-3
3,3-dimethyl-1-(phenylthio)butan-2-one

: 137351-35-0
3,3-dimethyl β-keto α-thiophenyl butyl p-toluene sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro succinimide / CCl₄ / 2 h / 0 °C

2: 59 percent / tetrabutylammonium hydrogen sulphate / acetone; benzene / 4 h / 60 °C

With N-chloro-succinimide; tetra(n-butyl)ammonium hydrogensulfate; In tetrachloromethane; acetone; benzene;
DOI:10.1080/00397919108019810