[(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄)

Base Information

• Chemical Name: [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄)
• CAS No.: 1428241-02-4
• Molecular Formula: C₃₆H₅₈Cu₂N₈O₆S₂*O₄S
• Molecular Weight: 986.194

Synonyms:[(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄)

Chemical Property of [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄)

Chemical Property:

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Technology Process of [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄)

There total 3 articles about [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone^(1-))2(triethylamine)2(H₂O)4](SO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

copper(ll) sulfate pentahydrate + (E)-2-(furan-2-ylmethylene)-N-phenylhydrazine-1-carbothioamide (920339-22-6) + triethylamine (121-44-8) → [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone(1-))2(triethylamine)2(H2O)4](SO4) (1428241-02-4)

Guidance literature:

In ethanol; at 20 ℃; for 8h; Reflux;

DOI:10.1016/j.poly.2012.12.030

Reference yield:

4-Phenyl-3-thiosemicarbazide (5351-69-9) → [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone(1-))2(triethylamine)2(H2O)4](SO4) (1428241-02-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 8 h / 20 °C / Reflux

2: ethanol / 8 h / 20 °C / Reflux

In ethanol;

DOI:10.1016/j.poly.2012.12.030

Reference yield:

furfural (98-01-1) → [(copper(II))2(2-furaldehyde-4-phenylisothiosemicarbazone(1-))2(triethylamine)2(H2O)4](SO4) (1428241-02-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 8 h / 20 °C / Reflux

2: ethanol / 8 h / 20 °C / Reflux

In ethanol;

DOI:10.1016/j.poly.2012.12.030

upstream raw materials:

(E)-2-(furan-2-ylmethylene)-N-phenylhydrazine-1-carbothioamide

triethylamine

4-Phenyl-3-thiosemicarbazide

furfural

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