5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene

Base Information

• Chemical Name: 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene
• CAS No.: 1017967-78-0
• Molecular Formula: C₂₈H₄₉BrO₁₂
• Molecular Weight: 657.594
• Mol file: 1017967-78-0.mol

Synonyms:5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene

Chemical Property of 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene

There total 6 articles about 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-phenyl)methanol (885473-88-1) → 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene (1017967-78-0)

Guidance literature:

With phosphorus tribromide; In dichloromethane; at 0 ℃;

DOI:10.1039/C8SC02882F

Reference yield:

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate (62921-74-8,518012-62-9,58320-73-3) → 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene (1017967-78-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile

2: lithium aluminium tetrahydride / tetrahydrofuran

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetonitrile;

DOI:10.1021/ja5093503

Reference yield:

Ethyl gallate (831-61-8) → 5-(bromomethyl)-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene (1017967-78-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile

2: lithium aluminium tetrahydride / tetrahydrofuran

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetonitrile;

DOI:10.1021/ja5093503

upstream raw materials:

trimethylsilyl bromide

Ethyl gallate

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-phenyl)methanol

Downstream raw materials:

C₃₀H₅₂O₁₃S

(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)methanethiol

2,5-bis(3,4,5-tris (2-(2-(2-methoxy-ethoxy)ethoxy)ethoxy)benzyloxy)-1,4-dibromobenzene

C₁₁₆H₁₄₄N₆O₃₄