(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

Base Information

Chemical Name:(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate
CAS No.:156943-61-2
Molecular Formula:C₁₇H₂₅NO₂S₂
Molecular Weight:339.523
Hs Code.:

Synonyms:(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

Chemical Property:

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Technology Process of (+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

There total 3 articles about (+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19009-39-3
N,N-diisopropylcarbamoyl chloride

: 156943-61-2
(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 10 h / 90 °C

2: 1) s-BuLi, TMEDA

With pyridine; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium;
DOI:10.1016/S0040-4020(01)90461-2

Reference yield:

: 1445-91-6
(S)-1-phenylethanol

: 156943-61-2
(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 10 h / 90 °C

2: 1) s-BuLi, TMEDA

With pyridine; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium;
DOI:10.1016/S0040-4020(01)90461-2

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 133038-74-1
(S)-(-)-1-phenylethyl N,N-diisopropylcarbamate

: 74-88-4
methyl iodide

: 156943-61-2
(+)-(R)-S-methyl (R)-2-(N,N-diisopropylcarbamoyloxy)-2-methylpropanedithioate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction;
DOI:10.1016/S0040-4020(01)90461-2