3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

Base Information

Chemical Name:3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin
CAS No.:1332462-77-7
Molecular Formula:C₁₇H₁₂ClN₅O₂
Molecular Weight:353.768
Hs Code.:

Synonyms:3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

Chemical Property:

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Technology Process of 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

There total 4 articles about 3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 147440-65-1
4-amino-3-(p-chlorobenzyl)-1H-1,2,4-triazol-5-one

: 1332462-77-7
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

Guidance literature:: With acetic acid; In ethanol; at 110 ℃; for 0.0833333h; Microwave irradiation; Closed vessel;
DOI:10.3184/174751911X13043524455143

Reference yield:

: 42366-35-8,1769-41-1
hydroxyimino-N-phenylacetamide

: 1332462-77-7
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: acetic acid / ethanol / 0.08 h / 110 °C / Microwave irradiation; Closed vessel

With acetic acid; In ethanol;
DOI:10.3184/174751911X13043524455143

Reference yield:

: 141525-15-7
ethyl 2-[2-(4-chlorophenyl)-1-ethoxyethylidene]hydrazinecarboxylate

: 1332462-77-7
3-[5'-(4''-chlorobenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]iminoisatin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water / 0.05 h / 90 °C / Microwave irradiation; Closed vessel

2: acetic acid / ethanol / 0.08 h / 110 °C / Microwave irradiation; Closed vessel

With hydrazine hydrate; acetic acid; In ethanol; water;
DOI:10.3184/174751911X13043524455143