3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

Base Information

Chemical Name:3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside
CAS No.:1403890-30-1
Molecular Formula:C₂₈H₃₂N₂O₉
Molecular Weight:540.57
Hs Code.:

Synonyms:3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

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Chemical Property of 3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

Chemical Property:

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Technology Process of 3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

There total 4 articles about 3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(benzyloxycarbonyl)aminopropyl 2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 1403890-30-1
3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; for 3h;
DOI:10.1016/j.bmc.2012.08.048

Reference yield:

: 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-galactopyranosyl trichloroacetimidate

: 1403890-30-1
3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Molecular sieve

2: sodium methylate / methanol / 12 h / pH 10

3: toluene-4-sulfonic acid / 3 h

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2012.08.048

Reference yield:

: 1403890-29-8
3-(benzyloxycarbonyl)aminopropyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-galactopyranoside

: 1403890-30-1
3-(benzyloxycarbonyl)aminopropyl 2-deoxy-3,4-O-isopropylidene-2-phthalimido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 12 h / pH 10

2: toluene-4-sulfonic acid / 3 h

With sodium methylate; toluene-4-sulfonic acid; In methanol;
DOI:10.1016/j.bmc.2012.08.048