C₂₃H₁₈N₂O₅

Base Information

Chemical Name:C₂₃H₁₈N₂O₅
CAS No.:1380109-92-1
Molecular Formula:C₂₃H₁₈N₂O₅
Molecular Weight:402.406
Hs Code.:

C<sub>23</sub>H<sub>18</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₃H₁₈N₂O₅

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Chemical Property of C₂₃H₁₈N₂O₅

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Technology Process of C₂₃H₁₈N₂O₅

There total 5 articles about C₂₃H₁₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1380109-91-0
C₂₄H₂₀N₂O₅

: 1380109-92-1
C₂₃H₁₈N₂O₅

Guidance literature:: C₂₄H₂₀N₂O₅; With water; lithium hydroxide; In tetrahydrofuran; methanol; at 20 - 25 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=3;

Reference yield:

: 112334-42-6
benzyl 4,5-bis(benzyloxy)picolinate

: 1380109-92-1
C₂₃H₁₈N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

1.2: -78 - 25 °C

2.1: hydroxylamine hydrochloride; sodium acetate / methanol / 3 h / Reflux

3.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.5 h / 55 °C

3.2: 0 - 5 °C

4.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 20 - 25 °C

4.2: pH 3

With pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; diisobutylaluminium hydride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 1380109-90-9
C₂₀H₁₈N₂O₃

: 1380109-92-1
C₂₃H₁₈N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.5 h / 55 °C

1.2: 0 - 5 °C

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 20 - 25 °C

2.2: pH 3

With pyridine; N-chloro-succinimide; water; lithium hydroxide; In tetrahydrofuran; methanol;