N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

Base Information

Chemical Name:N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide
CAS No.:350671-22-6
Molecular Formula:C₂₅H₂₁N₇O₅
Molecular Weight:499.486
Hs Code.:

Synonyms:N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

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Chemical Property of N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

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Technology Process of N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

There total 3 articles about N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

: 141-86-6
2.6-diaminopyridine

: 350671-21-5
Diethyl 5-(4-nitrophenylmethyloxy)isophthalate

: 350671-22-6
N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

Guidance literature:: 2.6-diaminopyridine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

Diethyl 5-(4-nitrophenylmethyloxy)isophthalate; In tetrahydrofuran; hexane; at -78 - -60 ℃; for 6h;
DOI:10.1055/s-2001-13392

Reference yield:

: 618-83-7
5-Hydroxyisophthalic acid

: 350671-22-6
N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / AcCl / 4 h / Heating

2.1: 96.5 percent / K₂CO₃ / acetone / 2 h / Heating

3.1: n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C

3.2: 90.9 percent / tetrahydrofuran; hexane / 6 h / -78 - -60 °C

With n-butyllithium; potassium carbonate; acetyl chloride; In tetrahydrofuran; hexane; acetone;
DOI:10.1055/s-2001-13392

Reference yield:

: 39630-68-7
diethyl 5-hydroxyisophthalate

: 350671-22-6
N,N'-Bis[2-(6-aminopyridyl)]-5-(4-nitrophenylmethyloxy)isophthaldiamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96.5 percent / K₂CO₃ / acetone / 2 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.2: 90.9 percent / tetrahydrofuran; hexane / 6 h / -78 - -60 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; acetone;
DOI:10.1055/s-2001-13392