μ-1,2-trimethylene-o-carborane

Base Information

Chemical Name:μ-1,2-trimethylene-o-carborane
CAS No.:23940-20-7
Molecular Formula:C₅H₁₆B₁₀
Molecular Weight:184.292
Hs Code.:

Synonyms:μ-1,2-trimethylene-o-carborane

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Chemical Property of μ-1,2-trimethylene-o-carborane

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Technology Process of μ-1,2-trimethylene-o-carborane

There total 1 articles about μ-1,2-trimethylene-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: [nido-(CH₂)3C₂B₁₀H₁₀][Na₂(THF)x]

: 873-51-8
phenylborondichloride

: 23940-20-7
μ-1,2-trimethylene-o-carborane

: 1,2-(CH₂)3-3-Ph-1,2-C₂B₁₁H₁₀

Guidance literature:: In toluene; (N2); slow addn. of dihaloborane to a suspn. of boron compd. in toluene at -78°C, stirring for 1 h, stirring at room temp. for 6 h; chromy. (SiO2, n-hexane);
DOI:10.1021/ja0605772

Reference yield: 98.0%

: 23940-20-7
μ-1,2-trimethylene-o-carborane

: 13400-13-0
cesium fluoride

: 89462-13-5
Cs[μ-7,8-trimethylene-7,8-C2B9H10]

: 7637-07-2
boron trifluoride

: 13842-55-2
boron difluoride

Guidance literature:: In ethanol; under N2; mixt. of B compd. and CsF (molar ratio 1:3) in EtOH stirred under reflux for 25 h; cooled to room temp.; dried in vac. by rotary evaporator; dissolved in acetone; filtered by glass frit; washed with acetone; solvent removed from filtrate in vac.; recrystd. from H2O; elem. anal.;
DOI:10.1021/ic000768k