C₃₃H₃₁F₃O₇S

Base Information

Chemical Name:C₃₃H₃₁F₃O₇S
CAS No.:1394902-96-5
Molecular Formula:C₃₃H₃₁F₃O₇S
Molecular Weight:628.666
Hs Code.:

C<sub>33</sub>H<sub>31</sub>F<sub>3</sub>O<sub>7</sub>S

Synonyms:C₃₃H₃₁F₃O₇S

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Chemical Property of C₃₃H₃₁F₃O₇S

Chemical Property:

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Technology Process of C₃₃H₃₁F₃O₇S

There total 11 articles about C₃₃H₃₁F₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1394902-95-4
C₃₂H₃₂O₅

: 1394902-96-5
C₃₃H₃₁F₃O₇S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere; Reflux;
DOI:10.1021/ol302132s

Reference yield:

: 1394902-93-2
C₁₆H₂₅BO₅

: 1394902-96-5
C₃₃H₃₁F₃O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 16 h / 105 °C / Inert atmosphere

2: 5% Pd/C; triethylamine; hydrogen / ethyl acetate / 24 h / 2250.23 Torr

3: hydrogenchloride / tetrahydrofuran / 16 h / 20 °C

4: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Reflux

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 5% Pd/C; potassium tert-butylate; hydrogen; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol302132s

Reference yield:

: C₉H₁₁BrO₃

: 1394902-96-5
C₃₃H₃₁F₃O₇S

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / acetone / 3 h / Inert atmosphere; Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C

3.1: potassium dihydrogenphosphate / water; diethyl ether / Inert atmosphere

4.1: magnesium sulfate / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 16 h / 105 °C / Inert atmosphere

6.1: 5% Pd/C; triethylamine; hydrogen / ethyl acetate / 24 h / 2250.23 Torr

7.1: hydrogenchloride / tetrahydrofuran / 16 h / 20 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Reflux

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Reflux

With hydrogenchloride; potassium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 5% Pd/C; potassium tert-butylate; hydrogen; sodium carbonate; magnesium sulfate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol302132s