tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

Base Information

Chemical Name:tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate
CAS No.:1305311-04-9
Molecular Formula:C₂₃H₃₇N₃O₄
Molecular Weight:419.564
Hs Code.:

Synonyms:tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

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Chemical Property of tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

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Technology Process of tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

There total 5 articles about tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1305311-00-5
tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-N-hydroxy-3-methylbutanimidoyl]amino}-3-phenylpropionate

: 1305311-04-9
tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

Guidance literature:: With hydrogen; In methanol; water; acetic acid; at 20 ℃; for 1h;
DOI:10.1039/c0ob01193b

Reference yield:

: 175666-90-7
tert-butyl [(S)-1-(hydroxyiminomethyl)-2-methylpropyl]carbamate

: 1305311-04-9
tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C

2: triethylamine / diethyl ether / 20 °C

3: hydrogen / methanol; water; acetic acid / 1 h / 20 °C

With N-chloro-succinimide; hydrogen; triethylamine; In methanol; diethyl ether; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01193b

Reference yield:

: 331779-00-1
(S)-tert-butyl N-[1-chloro-1-(hydroxyimino)-3-methylbutan-2-yl]carbamate

: 1305311-04-9
tert-butyl (S)-2-{[(S)-2-tert-butoxycarbonylamino-3-methylbutanimidoyl]amino}-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 20 °C

2: hydrogen / methanol; water; acetic acid / 1 h / 20 °C

With hydrogen; triethylamine; In methanol; diethyl ether; water; acetic acid;
DOI:10.1039/c0ob01193b