C₂₄H₂₆N₂O₃

Base Information

Chemical Name:C₂₄H₂₆N₂O₃
CAS No.:1448802-15-0
Molecular Formula:C₂₄H₂₆N₂O₃
Molecular Weight:390.482
Hs Code.:

C<sub>24</sub>H<sub>26</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₆N₂O₃

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Chemical Property of C₂₄H₂₆N₂O₃

Chemical Property:

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Technology Process of C₂₄H₂₆N₂O₃

There total 7 articles about C₂₄H₂₆N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: C₂₄H₂₆N₂O₃

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 1448802-16-1
C₂₄H₂₆N₂O₃

Guidance literature:: With Daicel Chiral-Pak AS; In ethanol; hexane; diethylamine; Resolution of racemate;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₈H₃₀N₂O₅S₂

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 1448802-16-1
C₂₄H₂₆N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1 h / 110 °C

2.1: lithium hydroxide monohydrate / methanol; tetrahydrofuran; water / 50 °C

3.1: triethylamine; diphenyl phosphoryl azide / toluene; acetonitrile / 1.5 h / 30 °C

3.2: 2 h / 120 °C

4.1: triethylamine; lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

5.1: trimethyl(benzyl)ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

6.1: diethylamine / ethanol; hexane / Resolution of racemate

With lithium hydroxide monohydrate; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tri-n-butyl-tin hydride; trimethyl(benzyl)ammonium fluoride; diethylamine; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; hexane; water; toluene; acetonitrile;
DOI:10.1002/chem.201604647

Reference yield:

: C₂₆H₂₈N₂O₄

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 1448802-16-1
C₂₄H₂₆N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide monohydrate / methanol; tetrahydrofuran; water / 50 °C

2.1: triethylamine; diphenyl phosphoryl azide / toluene; acetonitrile / 1.5 h / 30 °C

2.2: 2 h / 120 °C

3.1: triethylamine; lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

4.1: trimethyl(benzyl)ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

5.1: diethylamine / ethanol; hexane / Resolution of racemate

With lithium hydroxide monohydrate; diphenyl phosphoryl azide; trimethyl(benzyl)ammonium fluoride; diethylamine; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; hexane; water; toluene; acetonitrile;
DOI:10.1002/chem.201604647