1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

Base Information

Chemical Name:1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol
CAS No.:1585977-91-8
Molecular Formula:C₂₄H₃₅NO₇
Molecular Weight:449.544
Hs Code.:

Synonyms:1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

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Technology Process of 1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

There total 1 articles about 1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1585977-90-7
C₁₈H₂₉NO₄

: 108-24-7
acetic anhydride

: 1585977-91-8
1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

Guidance literature:: With pyridine; In 1,4-dioxane; at 20 ℃; for 17h;
DOI:10.1016/j.tetasy.2014.01.014

Reference yield: 100.0%

: 1585977-91-8
1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

: 1585977-90-7
C₁₈H₂₉NO₄

Guidance literature:: With sodium methylate; In methanol; at 40 ℃; for 16h;
DOI:10.1016/j.tetasy.2014.01.014

Reference yield:

: 1585977-91-8
1,5,6-tri-O-acetyl-3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-talitol

: 1585977-92-9
methyl 3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 16 h / 40 °C

2: sodium periodate / 1,4-dioxane; water / 1 h / 0 °C

3: potassium carbonate; iodine / 2 h / 0 °C / Inert atmosphere

With sodium periodate; iodine; sodium methylate; potassium carbonate; In 1,4-dioxane; methanol; water;
DOI:10.1016/j.tetasy.2014.01.014