N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

Base Information

Chemical Name:N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid
CAS No.:1585977-94-1
Molecular Formula:C₁₀H₁₉NO₄
Molecular Weight:217.265
Hs Code.:

Synonyms:

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Chemical Property of N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

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Technology Process of N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

There total 12 articles about N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1585977-93-0
3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

: 1585977-94-1
N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

Guidance literature:: With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In 1,4-dioxane; water; at 20 ℃; for 3h;
DOI:10.1016/j.tetasy.2014.01.014

Reference yield:

: methyl 3-O-benzyl-N-butyl-2,4-dideoxy-2,4-imino-6-O-trityl-β-d-talopyranoside

: 1585977-94-1
N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

Guidance literature:: Multi-step reaction with 9 steps

1.1: palladium 10% on activated carbon; ammonium formate / methanol / 0.5 h / Inert atmosphere; Reflux

2.1: Dess-Martin periodane / dichloromethane / 20 h / 0 - 20 °C

3.1: diethyl ether / 2 h / -78 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 0 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / 1,4-dioxane / 17 h / 50 °C

5.2: 18 h / 20 °C

6.1: sodium periodate / 1,4-dioxane; water / 1 h / 0 °C

7.1: potassium carbonate; iodine / 2 h / 0 °C / Inert atmosphere

8.1: potassium carbonate / 1,4-dioxane; water / 23 h / 65 °C

9.1: palladium 10% on activated carbon; hydrogenchloride; hydrogen / 1,4-dioxane; water / 3 h / 20 °C

With hydrogenchloride; sodium periodate; palladium 10% on activated carbon; hydrogen; iodine; ammonium formate; sodium hydride; potassium carbonate; Dess-Martin periodane; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tetasy.2014.01.014

Reference yield:

: methyl N-butyl-2,4-dideoxy-2,4-imino-6-O-trityl-β-d-lyxo-hexopyranoside-3-ulose

: 1585977-94-1
N-butyl-2,4-dideoxy-2,4-imino-3-methyl-d-ribonic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether / 2 h / -78 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 0 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 17 h / 50 °C

3.2: 18 h / 20 °C

4.1: sodium periodate / 1,4-dioxane; water / 1 h / 0 °C

5.1: potassium carbonate; iodine / 2 h / 0 °C / Inert atmosphere

6.1: potassium carbonate / 1,4-dioxane; water / 23 h / 65 °C

7.1: palladium 10% on activated carbon; hydrogenchloride; hydrogen / 1,4-dioxane; water / 3 h / 20 °C

With hydrogenchloride; sodium periodate; palladium 10% on activated carbon; hydrogen; iodine; sodium hydride; potassium carbonate; In 1,4-dioxane; diethyl ether; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tetasy.2014.01.014