N--N-methyl-anilin

Base Information

• Chemical Name: N--N-methyl-anilin
• CAS No.: 10469-34-8
• Molecular Formula: C₉H₉ClFNO
• Molecular Weight: 201.628

Synonyms:N--N-methyl-anilin

Chemical Property of N--N-methyl-anilin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N--N-methyl-anilin

There total 4 articles about N--N-methyl-anilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl chlorofluoroacetate (433-52-3,25197-79-9) + lithium N-methylanilide (35954-01-9) → N--N-methyl-anilin (10469-34-8)

Guidance literature:

at -78 ℃;

DOI:10.1021/jo00082a018

Reference yield:

N-Methyl-N-<2-chlor-1.2-difluor-vinyl>-anilin (2588-70-7) → N--N-methyl-anilin (10469-34-8)

Guidance literature:

With sulfuric acid;

Reference yield:

N-methylaniline (100-61-8) → N--N-methyl-anilin (10469-34-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) Li, styrene, (ii) /BRN= 1740373/

2: aq. H₂SO₄

With sulfuric acid;

upstream raw materials:

N-Methyl-N-<2-chlor-1.2-difluor-vinyl>-anilin

chlorofluoroacetyl chloride

N-methylaniline

methyl chlorofluoroacetate

Downstream raw materials:

N-(2-Chloro-2-fluoroethyl)-N-methylaniline

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