C₄₅H₄₂F₅N₅O₁₈S₂

Base Information

Chemical Name:C₄₅H₄₂F₅N₅O₁₈S₂
CAS No.:178447-05-7
Molecular Formula:C₄₅H₄₂F₅N₅O₁₈S₂
Molecular Weight:1099.98
Hs Code.:

C<sub>45</sub>H<sub>42</sub>F<sub>5</sub>N<sub>5</sub>O<sub>18</sub>S<sub>2</sub>

Synonyms:C₄₅H₄₂F₅N₅O₁₈S₂

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Chemical Property of C₄₅H₄₂F₅N₅O₁₈S₂

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Technology Process of C₄₅H₄₂F₅N₅O₁₈S₂

There total 7 articles about C₄₅H₄₂F₅N₅O₁₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 189624-31-5
C₅₂H₄₆F₅N₅O₁₈S₂

: 178447-05-7
C₄₅H₄₂F₅N₅O₁₈S₂

Guidance literature:: With acetic acid; at 70 ℃; for 7h;
DOI:10.1039/p19960000985

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 178447-05-7
C₄₅H₄₂F₅N₅O₁₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / DCC / ethyl acetate / Ambient temperature

2: 98 percent / molecular sieves 4 Angstroem, TMSOTf / CH₂Cl₂ / 1.) 0 deg C, 10 min, 2.) 0 deg C, 30 min

3: 98 percent / 80percent aq. AcOH / 7 h / 70 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;
DOI:10.1039/p19960000985

Reference yield:

: 120791-77-7
N-(9H-fluoren-9-yl)-methoxycarbonyl-O-(3,4,6-tri-O-acetyl-2-azido-2-desoxy-α-D-galactopyranosyl)-1-threonine tert-butyl ester

: 178447-05-7
C₄₅H₄₂F₅N₅O₁₈S₂

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / HCO₂H / 12 h / Ambient temperature

2: 65 percent / N₂H₄*H₂O / methanol / 7.5 h / Ambient temperature

3: 73 percent / p-TsOH / nitromethane / 3 h / Ambient temperature

4: 75 percent / DCC / ethyl acetate / Ambient temperature

5: 98 percent / molecular sieves 4 Angstroem, TMSOTf / CH₂Cl₂ / 1.) 0 deg C, 10 min, 2.) 0 deg C, 30 min

6: 98 percent / 80percent aq. AcOH / 7 h / 70 °C

With formic acid; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; In methanol; nitromethane; dichloromethane; ethyl acetate;
DOI:10.1039/p19960000985