N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide

Base Information

• Chemical Name: N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide
• CAS No.: 1005420-45-0
• Molecular Formula: C₁₅H₉F₄N₃O₂S
• Molecular Weight: 371.315
• Mol file: 1005420-45-0.mol

Synonyms:N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide

Chemical Property of N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide

There total 2 articles about N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,3,4,5-tetrafluorobenzoyl isothiocyanate (950725-15-2) + benzoic acid hydrazide (613-94-5) → N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide (1005420-45-0)

Guidance literature:

In acetonitrile; for 1h; Heating;

DOI:10.1134/S1070428007010083

Reference yield:

2,3,4,5-tetrafluorobenzoyl chloride (94695-48-4) → N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide (1005420-45-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile; toluene / 0.08 h / 40 °C

2: 92 percent / acetonitrile / 1 h / Heating

In toluene; acetonitrile;

DOI:10.1134/S1070428007010083

Reference yield: 92.0%

N-(2-benzoylhydrazinocarbothioyl)-2,3,4,5-tetrafluorobenzamide (1005420-45-0) → 7,8,9-trifluoro-2-phenyl-5H-[1,3,4]thiadiazolo[3,2-a]quinazolin-5-one

Guidance literature:

In diphenylether; biphenyl; for 12h; Reflux;

DOI:10.1134/S1070428019010093

upstream raw materials:

2,3,4,5-tetrafluorobenzoyl isothiocyanate

benzoic acid hydrazide

2,3,4,5-tetrafluorobenzoyl chloride