N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane

Base Information

• Chemical Name: N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane
• CAS No.: 860777-96-4
• Molecular Formula: C₁₉H₂₄N₂O₂
• Molecular Weight: 312.412
• Mol file: 860777-96-4.mol

Synonyms:N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane

Chemical Property of N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane

Chemical Property:

Purity/Quality:

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Technology Process of N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane

There total 2 articles about N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1,4-Diazacycloheptane (505-66-8) + 2-(bromomethyl)phenyl acetate (704-65-4) → N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane (860777-96-4)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 72h; pH=7 - 8;

DOI:10.1002/ejic.200400618

Reference yield:

1,4-Diazacycloheptane (505-66-8) + salicylaldehyde (90-02-8) → N,N''-bis(2-hydroxybenzyl)-1,4-diazacycloheptane (860777-96-4)

Guidance literature:

With sodium cyanoborohydride; acetic acid;

DOI:10.1002/chem.201001177

upstream raw materials:

1,4-Diazacycloheptane

2-(bromomethyl)phenyl acetate

salicylaldehyde