ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside
CAS No.:303775-64-6
Molecular Formula:C₃₅H₃₇IO₁₀S
Molecular Weight:776.643
Hs Code.:

Synonyms:ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

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Chemical Property of ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

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Technology Process of ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

There total 3 articles about ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 123-76-2
levulinic acid

: 303775-62-4
ethyl 2,6-di-O-benzoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 303775-64-6
ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(00)00612-8

Reference yield:

: 529-28-2
4-iodoanisol

: 303775-64-6
ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 74 percent / acetic acid / 60 h / 55 °C

2.1: dibutyltin oxide / toluene / 7 h / Heating

2.2: 60 percent / cesium fluoride / dimethylformamide / 7 h / 55 °C

3.1: 84 percent / DCC; DMAP / tetrahydrofuran

With dmap; di(n-butyl)tin oxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; acetic acid; toluene; 1.1: Substitution / 2.1: cyclocondensation / 2.2: Alkylation / 3.1: Acylation;
DOI:10.1016/S0040-4020(00)00612-8

Reference yield:

: 143191-43-9
3-iodo-4-methoxybenzyl chloride

: 303775-64-6
ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-(3-iodo-4-methoxybenzyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dibutyltin oxide / toluene / 7 h / Heating

1.2: 60 percent / cesium fluoride / dimethylformamide / 7 h / 55 °C

2.1: 84 percent / DCC; DMAP / tetrahydrofuran

With dmap; di(n-butyl)tin oxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; toluene; 1.1: cyclocondensation / 1.2: Alkylation / 2.1: Acylation;
DOI:10.1016/S0040-4020(00)00612-8