2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

Base Information

Chemical Name:2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde
CAS No.:1150111-59-3
Molecular Formula:C₁₈H₁₈N₂O₄
Molecular Weight:326.352
Hs Code.:

Synonyms:2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

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Chemical Property of 2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

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Technology Process of 2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

There total 1 articles about 2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 110-91-8,99108-56-2
morpholine

: 1150111-57-1
4-[(5-formyl-6-methyl-2-pyridinyl)oxy]benzoic acid

: 1150111-59-3
2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

Guidance literature:: 4-[(5-formyl-6-methyl-2-pyridinyl)oxy]benzoic acid; With 1,1'-carbonyldiimidazole; In acetonitrile; at 77 ℃; for 2h;

morpholine; In acetonitrile; at 20 ℃; for 0.25h;

Reference yield: 62.0%

: 1150111-59-3
2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

: 1150103-10-8
5-({[(3-fluorophenyl)(4-piperidinyl)amino]carbonyl}amino)-2-pyridinecarboxamide

: 64-19-7,77671-22-8
acetic acid

: 5-{[((3-fluorophenyl){1-[(2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinyl)methyl]-4-piperidinyl}amino)carbonyl]amino}-2-pyridinecarboxamide acetate

Guidance literature:: 2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde; 5-({[(3-fluorophenyl)(4-piperidinyl)amino]carbonyl}amino)-2-pyridinecarboxamide; With sodium tris(acetoxy)borohydride; In dichloromethane; for 16h;

With water; potassium carbonate; In dichloromethane;

acetic acid; In ethyl acetate;

Reference yield: 59.0%

: 1150111-59-3
2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde

: N-(3-fluorophenyl)-N-(4-fluorophenyl)-N-4-piperidinylurea hydrochloride

: 1150111-49-1
N-(3-fluorophenyl)-N'-(4-fluorophenyl)-N-{1-[(2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinyl)methyl]-4-piperidinyl}urea

Guidance literature:: 2-methyl-6-{[4-(4-morpholinylcarbonyl)phenyl]oxy}-3-pyridinecarbaldehyde; N-(3-fluorophenyl)-N-(4-fluorophenyl)-N-4-piperidinylurea hydrochloride; With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 16h;

With water; potassium carbonate; In dichloromethane;