2-phenylpenta-3,4-dien-2-amine

Base Information

Chemical Name:2-phenylpenta-3,4-dien-2-amine
CAS No.:1221894-71-8
Molecular Formula:C₁₁H₁₃N
Molecular Weight:159.231
Hs Code.:

Synonyms:2-phenylpenta-3,4-dien-2-amine

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Chemical Property of 2-phenylpenta-3,4-dien-2-amine

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Technology Process of 2-phenylpenta-3,4-dien-2-amine

There total 6 articles about 2-phenylpenta-3,4-dien-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: trans-3-ethynyl-2-methyl-2-phenylaziridine

: 1221894-71-8
2-phenylpenta-3,4-dien-2-amine

Guidance literature:: trans-3-ethynyl-2-methyl-2-phenylaziridine; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200906066

Reference yield:

: C₁₂H₁₅N₃O₃

: 1221894-71-8
2-phenylpenta-3,4-dien-2-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine / acetonitrile / 50 - 83 °C

2.1: diisobutylaluminium hydride / toluene / -78 °C

3.1: potassium carbonate / methanol / 8 h / 20 °C / Inert atmosphere

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; potassium carbonate; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; methanol; toluene; acetonitrile; 3.1: Wittig-type reaction;
DOI:10.1002/anie.200906066

Reference yield:

: 77-83-8,19464-92-7,19464-95-0,33530-46-0,59492-57-8,59492-58-9,70774-46-8,72691-66-8,72691-67-9
ethyl (E)-3-methyl-3-phenylglycidate

: 1221894-71-8
2-phenylpenta-3,4-dien-2-amine

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide; ammonium chloride / ethanol / 8 h / 80 °C

2.1: triphenylphosphine / acetonitrile / 50 - 83 °C

3.1: diisobutylaluminium hydride / toluene / -78 °C

4.1: potassium carbonate / methanol / 8 h / 20 °C / Inert atmosphere

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

With sodium azide; diisobutylaluminium hydride; potassium carbonate; ammonium chloride; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; toluene; acetonitrile; 4.1: Wittig-type reaction;
DOI:10.1002/anie.200906066