(4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol

Base Information

• Chemical Name: (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol
• CAS No.: 137157-07-4
• Molecular Formula: C₂₄H₂₄N₅O₆P
• Molecular Weight: 509.458

Synonyms:(4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol

Chemical Property of (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol

Chemical Property:

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Technology Process of (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol

There total 3 articles about (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

benzyl bromide (100-39-0) + C22H38N6O6P(1+) → (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinine-2,7-diol (55053-32-2) + (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol (137157-07-4)

Guidance literature:

In N,N-dimethyl acetamide; 1.) 50-60 deg C, 6 h, 2.) RT, 2 d;

DOI:10.3987/COM-91-5750

Reference yield: 34.0%

benzyl bromide (100-39-0) + C22H38N6O6P(1+) → (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol (137157-07-4) + cAMP benzyl ester (62742-71-6)

Guidance literature:

In N,N-dimethyl acetamide; 1.) 50-60 deg C, 6 h, 2.) RT, 2 d;

DOI:10.3987/COM-91-5750

Reference yield: 0.7%

benzyl bromide (100-39-0) + C22H38N6O6P(1+) → (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinine-2,7-diol (55053-32-2) + (4aR,6R,7R,7aS)-6-(1-Benzyl-6-imino-1,6-dihydro-purin-9-yl)-2-benzyloxy-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinin-7-ol (137157-07-4) + cAMP (60-92-4) + cAMP benzyl ester (62742-71-6)

Guidance literature:

With sodium carbonate; In N,N-dimethyl acetamide; at 80 ℃; for 0.25h;

DOI:10.3987/COM-91-5750

upstream raw materials:

benzyl bromide

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