PHPh₂(2-BF₃-Ph)

Base Information

Chemical Name:PHPh₂(2-BF₃-Ph)
CAS No.:1318802-26-4
Molecular Formula:C₁₈H₁₄BF₃P*H
Molecular Weight:330.097
Hs Code.:

Synonyms:PHPh₂(2-BF₃-Ph)

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Chemical Property of PHPh₂(2-BF₃-Ph)

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Technology Process of PHPh₂(2-BF₃-Ph)

There total 5 articles about PHPh₂(2-BF₃-Ph) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1316853-58-3
ortho-(Ph₂P)C₆H₄(BF₃K)

: 1318802-26-4
PHPh₂(2-BF₃-Ph)

Guidance literature:: With tetrafluoroboric acid; In tetrahydrofuran; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/om2004095

Reference yield: 95.0%

: tetrafluoroboric acid

: K⁽¹⁺⁾*(C₆H₅)2PC₆H₄BF₃^(1-)=KBF₃C₆H₄P(C₆H₅)2

: 1318802-26-4
PHPh₂(2-BF₃-Ph)

Guidance literature:: In tetrahydrofuran; water; (inert atm, glovebox) a soln. of HBF4 in water was added to THF-soln. ofpotassium salt, stirring at room temp. for 2 h; volatiles were removed under reduced pressure, extd. with CHCl3, the solvent was removed under reduced pressure, recrystd. from hot acetonitrile; elem. anal.;
DOI:10.1021/om2004095

Reference yield:

: 734-59-8
(4-bromophenyl)diphenylphosphane

: 1318802-26-4
PHPh₂(2-BF₃-Ph)

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran

2: methanol; water

3: water; tetrahydrofuran

With n-butyllithium; In tetrahydrofuran; methanol; water;
DOI:10.1021/om2004095