N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide
CAS No.:1121746-86-8
Molecular Formula:C₂₁H₃₃NO₃SSi
Molecular Weight:407.649
Hs Code.:

Synonyms:N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

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Chemical Property of N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

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Technology Process of N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

There total 1 articles about N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 474022-55-4
[(5-bromo-4-pentyn-1-yl)oxy](tert-butyl)dimethyl-silane

: 1121746-86-8
N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; In toluene; at 75 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol802844z

Reference yield: 92.0%

: 110-91-8,99108-56-2
morpholine

: 1121746-86-8
N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

: C₂₂H₃₈N₂O₄SSi

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In tetrahydrofuran; at 80 ℃; Inert atmosphere;
DOI:10.1021/jo200780x

Reference yield: 90.0%

: 1121746-86-8
N-(but-3-en-1-yl)-N-(5-((tert-butyldimethylsilyl)oxy)pent-1-yn-1-yl)-4-methylbenzenesulfonamide

: 1443365-66-9
(Z)-2-(4-((tert-butyldimethylsilyl)oxy)butylidene)-3-methylene-1-tosylpyrrolidine

Guidance literature:: With N,N'-bis(benzyliden)ethylendiamine; palladium diacetate; In toluene; at 60 ℃; for 0.5h; Reagent/catalyst; Solvent; Time; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201304186