N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide
CAS No.:98809-71-3
Molecular Formula:C₁₈H₂₁NO₃S₃
Molecular Weight:395.568
Hs Code.:

Synonyms:N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

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Technology Process of N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

There total 5 articles about N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 34161-85-8
N-(2-formyl-4-methylphenyl)-4-methylbenzenesulfonamide

: 33577-16-1
methyl methylsulfinylmethyl sulfide

: 98809-71-3
N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; methanol; for 72h; Heating;

Reference yield:

: 34161-82-5
2-methoxycarbonyl-4-methyl-N-(p-toluenesulfonyl)aniline

: 98809-71-3
N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94.5 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

2: 93 percent / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h

3: 77 percent / Triton B / tetrahydrofuran; methanol / 72 h / Heating

With lithium aluminium tetrahydride; N-benzyl-trimethylammonium hydroxide; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 18595-16-9
2-amino-5-methylbenzoic acid methyl ester

: 98809-71-3
N-[2-((E)-2-Methanesulfinyl-2-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 3 h / 0 °C

2: 94.5 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

3: 93 percent / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h

4: 77 percent / Triton B / tetrahydrofuran; methanol / 72 h / Heating

With pyridine; lithium aluminium tetrahydride; N-benzyl-trimethylammonium hydroxide; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;