C₂₂H₃₆O₆Si

Base Information

Chemical Name:C₂₂H₃₆O₆Si
CAS No.:1394245-96-5
Molecular Formula:C₂₂H₃₆O₆Si
Molecular Weight:424.61
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>6</sub>Si

Synonyms:C₂₂H₃₆O₆Si

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Chemical Property of C₂₂H₃₆O₆Si

Chemical Property:

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Technology Process of C₂₂H₃₆O₆Si

There total 8 articles about C₂₂H₃₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₂O₆

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1394245-96-5
C₂₂H₃₆O₆Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; chemoselective reaction;
DOI:10.1016/j.tet.2012.06.105

Reference yield:

: 1394245-95-4
C₁₆H₁₈O₆

: 1394245-96-5
C₂₂H₃₆O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 - -40 °C

1.2: 13.5 h / -40 - 20 °C / Saturated solution

2.1: methanol; sodium tetrahydroborate / 1 h / 0 - 20 °C

2.2: Saturated solution

3.1: dmap; triethylamine / dichloromethane / 1 h / 0 - 20 °C

With methanol; dmap; sodium tetrahydroborate; diisobutylaluminium hydride; triethylamine; In dichloromethane; toluene;
DOI:10.1016/j.tet.2012.06.105

Reference yield:

: 103357-81-9,76542-57-9
5-O-trifluoromethanesulfonyl-1,2-O-isopropylidene-α-D-glucofuranurono-6,3-lactone

: 1394245-96-5
C₂₂H₃₆O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 18-crown-6 ether / N,N-dimethyl-formamide / 1 h / 0 °C

2.1: potassium carbonate / 2 h / -10 °C

2.2: Saturated solution

3.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 6 h / 80 °C

4.1: silver(l) oxide / ethyl acetate / 41 h / 0 - 50 °C

5.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 - -40 °C

5.2: 13.5 h / -40 - 20 °C / Saturated solution

6.1: methanol; sodium tetrahydroborate / 1 h / 0 - 20 °C

6.2: Saturated solution

7.1: dmap; triethylamine / dichloromethane / 1 h / 0 - 20 °C

With methanol; dmap; sodium tetrahydroborate; 18-crown-6 ether; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium carbonate; triethylamine; silver(l) oxide; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2012.06.105