3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

Base Information

Chemical Name:3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride
CAS No.:1310036-73-7
Molecular Formula:C₂₁H₁₉F₂NO₂*ClH
Molecular Weight:391.845
Hs Code.:

Synonyms:3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

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Chemical Property of 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

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Technology Process of 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

There total 1 articles about 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1310036-71-5
3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzonitrile

: 1310036-73-7
3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

Guidance literature:: 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzonitrile; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 2h;

With water; sodium hydroxide; In tetrahydrofuran; diethyl ether; for 0.166667h;

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; for 0.166667h;

Reference yield: 44.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1310036-73-7
3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

: 1310036-77-1
[3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamino]-acetic acid tert-butyl ester

Guidance literature:: bromoacetic acid tert-butyl ester; 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride; With triethylamine; In acetonitrile; for 15h; Reflux;

With hydrogenchloride; In diethyl ether;

Reference yield:

: 1310036-73-7
3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride

: 105-36-2
ethyl bromoacetate

: 1310036-75-9
[3-(4',5'-Difluoro-2'-methoxy-biphenyl-4-yloxymethyl)benzylamino]-acetic acid ethyl ester hydrochloride

Guidance literature:: 3-(4',5'-difluoro-2'-methoxy-biphenyl-4-yloxymethyl)-benzylamine hydrochloride; ethyl bromoacetate; With triethylamine; In acetonitrile; at 60 ℃; for 15h;

With hydrogenchloride; In diethyl ether;