C₅₅H₈₆O₁₁Si₂

Base Information

• Chemical Name: C₅₅H₈₆O₁₁Si₂
• CAS No.: 1283736-00-4
• Molecular Formula: C₅₅H₈₆O₁₁Si₂
• Molecular Weight: 979.452
• Mol file: 1283736-00-4.mol

Synonyms:C₅₅H₈₆O₁₁Si₂

Chemical Property of C₅₅H₈₆O₁₁Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₈₆O₁₁Si₂

There total 24 articles about C₅₅H₈₆O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.8%

C55H86O11Si2 (1283735-80-7) → C55H86O11Si2 (1283736-00-4)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃; for 3h;

DOI:10.1002/asia.201000882

Reference yield:

C21H30O3Si (1202747-69-0) → C55H86O11Si2 (1283736-00-4)

Guidance literature:

Multi-step reaction with 9 steps

1.1: 1H-imidazole; dmap / 0 - 20 °C

2.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.2: -78 - 20 °C

5.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C

6.1: dmap; triethylamine / dichloromethane / 20 °C

7.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 3 h / -78 °C / UV-irradiation

8.1: acetic acid; zinc / tetrahydrofuran / 10 h / 20 °C

9.1: hydrogenchloride / tetrahydrofuran; water / 3 h / 0 - 20 °C

With 1H-imidazole; hydrogenchloride; dmap; n-butyllithium; oxygen; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;

DOI:10.1002/asia.201000882

Reference yield:

C55H84O9Si2 (1283735-99-8) → C55H86O11Si2 (1283736-00-4)

Guidance literature:

Multi-step reaction with 3 steps

1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 3 h / -78 °C / UV-irradiation

2: acetic acid; zinc / tetrahydrofuran / 10 h / 20 °C

3: hydrogenchloride / tetrahydrofuran; water / 3 h / 0 - 20 °C

With hydrogenchloride; oxygen; 5,15,10,20-tetraphenylporphyrin; acetic acid; zinc; In tetrahydrofuran; dichloromethane; water;

DOI:10.1002/asia.201000882

upstream raw materials:

C₂₈H₃₆O₄Si

C₂₁H₃₀O₃Si

C₅₅H₈₄O₉Si₂

C₂₂H₃₄O₄