(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

Base Information

Chemical Name:(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol
CAS No.:170311-03-2
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

Synonyms:(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

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Chemical Property of (+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

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Technology Process of (+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

There total 3 articles about (+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 170311-02-1
(1'S,3'S)-(Z)-5-(1'-hydroxy-2',2'-dimethyl-6'-methylene-3'-tetrahydropyranyloxycyclohexyl)-3-methyl-2-penten-4-yn-1-yl-tetrahydropyranyl ether

: 170311-03-2
(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

Guidance literature:: With acetic acid; In tetrahydrofuran; water; for 48h; Ambient temperature;
DOI:10.1016/0031-9422(95)00374-G

Reference yield:

: 41967-81-1
(Z)-3-Methyl-2-penten-4-ynyl tetrahydropyranyl ether

: 170311-03-2
(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtBr, Mg / 1) THF, 0-5 deg C, 30 min, room temp. (30 min); 2) THF, room temp. overnight

2: 92 percent / HOAc / H₂O; tetrahydrofuran / 48 h / Ambient temperature

With ethidium Bromide; magnesium; acetic acid; In tetrahydrofuran; water;
DOI:10.1016/0031-9422(95)00374-G

Reference yield:

: (-)-(S)-2,2-dimethyl-6-methylene-3-tetrahydropyranoxy-1-cyclohexanone

: 170311-03-2
(+)-(1'S,3'S)-(Z)-5-(1',3'-dihydroxy-2',2'-dimethyl-6'-methylenecyclohexyl)-3-methyl-2-penten-4-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtBr, Mg / 1) THF, 0-5 deg C, 30 min, room temp. (30 min); 2) THF, room temp. overnight

2: 92 percent / HOAc / H₂O; tetrahydrofuran / 48 h / Ambient temperature

With ethidium Bromide; magnesium; acetic acid; In tetrahydrofuran; water;
DOI:10.1016/0031-9422(95)00374-G