2-fluoroisophthalic acid monooctyl ester

Base Information

Chemical Name:2-fluoroisophthalic acid monooctyl ester
CAS No.:640768-78-1
Molecular Formula:C₁₆H₂₁FO₄
Molecular Weight:296.339
Hs Code.:

Synonyms:2-fluoroisophthalic acid monooctyl ester

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Chemical Property of 2-fluoroisophthalic acid monooctyl ester

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Technology Process of 2-fluoroisophthalic acid monooctyl ester

There total 2 articles about 2-fluoroisophthalic acid monooctyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 111-87-5
octanol

: 1583-65-9
2-fluoro-isophthalic acid

: 640768-78-1
2-fluoroisophthalic acid monooctyl ester

Guidance literature:: With sulfuric acid; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/ja037312x

Reference yield:

: 443-88-9
2-fluoro-m-xylene

: 640768-78-1
2-fluoroisophthalic acid monooctyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / KMnO₄; cetyltrimethylammonium bromide / H₂O / 3 h / Heating

2: 49 percent / H₂SO₄ / tetrahydrofuran / 24 h / Heating

With potassium permanganate; sulfuric acid; cetyltrimethylammonim bromide; In tetrahydrofuran; water;
DOI:10.1021/ja037312x

Reference yield: 78.0%

: 497-18-7
carbonodihydrazide

: 640768-78-1
2-fluoroisophthalic acid monooctyl ester

: N',N'-(3-octyloxycarbonyl-2-fluorobenzoyl) carbonic dihydrazide

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; at 20 ℃; for 12h;
DOI:10.1021/ja037312x