6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Base Information

Chemical Name:6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene
CAS No.:1469857-75-7
Molecular Formula:C₂₁H₁₆N₂OS
Molecular Weight:344.437
Hs Code.:

Synonyms:6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Suppliers and Price of 6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

There total 7 articles about 6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: C₂₇H₃₀N₂O₂SSi

: 1469857-75-7
6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: With hydrogenchloride; In methanol; at 100 ℃; for 4h;

Reference yield:

: 1469858-12-5
6-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469857-75-7
6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; bromine / 12 h / 80 °C

2: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

3: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

4: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; bromine; sodium hydride; sodium carbonate; acetic acid; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;

Reference yield:

: 1469857-45-1
2-bromo-6-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469857-75-7
6-(4-methoxyphenyl)-2-phenyl-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

2: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

3: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium carbonate; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;