4-METHOXY-BENZOIC ACID PHENYL ESTER

Base Information

• Chemical Name: 4-METHOXY-BENZOIC ACID PHENYL ESTER
• CAS No.: 4181-97-9
• Molecular Formula: C14H12O3
• Molecular Weight: 228.247
• Hs Code.: 2918990090
• Mol file: 4181-97-9.mol

Synonyms:Benzoic acid,4-methoxy-,phenyl ester;p-Methoxybenzoic acid,phenyl ester;4-Methoxy-benzoic acid phenyl ester;phenyl-4-methoxybenzoate;phenyl p-methoxybenzoate;Benzoic acid, 4-methoxy-, phenyl ester;phenyl anisate;p-Anisic acid,phenyl ester;4-phenyl-4'-methoxybenzoate;

Chemical Property of 4-METHOXY-BENZOIC ACID PHENYL ESTER

Chemical Property:

• Vapor Pressure: 1.34E-05mmHg at 25°C
• Melting Point: 73.7 °C
• Boiling Point: 367.7°C at 760 mmHg
• Flash Point: 153.9°C
• PSA: 35.53000
• Density: 1.159g/cm³
• LogP: 2.91440
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: Chloroform (Slightly), DMSO (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

Phenyl4-Methoxybenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Phenyl 4-Methoxybenzoate is a useful reagent for the synthesis of pyrazoles via iodine catalyzed denitrative imino-diaza-Nazarov cyclization.Phenyl 4-Methoxybenzoate is a potent inhibitor of of 15-lipoxygenase.

Technology Process of 4-METHOXY-BENZOIC ACID PHENYL ESTER

There total 65 articles about 4-METHOXY-BENZOIC ACID PHENYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methoxy-benzaldehyde (123-11-5) + phenylboronic acid (98-80-6) → phenyl 4-methoxybenzoate (4181-97-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(mesityl)imidazolium chloride; In dimethyl sulfoxide; at 80 ℃; for 0.5h;

DOI:10.1002/asia.201200076

Reference yield: 97.0%

bis(phenyl) carbonate (102-09-0) + 4-methoxybenzoic acid (100-09-4) → phenyl 4-methoxybenzoate (4181-97-9)

Guidance literature:

With pyridine; dmap; at 20 ℃;

Reference yield: 96.0%

4-methoxybenzoic acid (100-09-4) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → phenyl 4-methoxybenzoate (4181-97-9)

Guidance literature:

With cesium fluoride; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1021/ol0361406

upstream raw materials:

4-methoxy-benzoyl chloride

phenol

4-methoxybenzoic acid

1,2-dihydro-2-phenoxycarbonylisoquinoline-1-carbonitrile

Downstream raw materials:

4,4'-Dihydroxybenzophenone

4-hydroxy-4'-methoxybenzophenone

1-(4-Methoxy-phenyl)-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethanone

phenolate

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