(1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

Base Information

Chemical Name:(1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol
CAS No.:1021954-55-1
Molecular Formula:C₃₁H₃₄O₄
Molecular Weight:470.609
Hs Code.:

Synonyms:(1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

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Technology Process of (1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

There total 1 articles about (1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1021954-56-2
C₃₀H₃₂Br₂O₄

: 74-88-4
methyl iodide

: 1021954-55-1
(1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

Guidance literature:: C₃₀H₃₂Br₂O₄; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -30 ℃; for 0.666667h;

methyl iodide; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jo702663w

Reference yield: 58.0%

: 1021954-55-1
(1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol

: 1021954-28-8
5,9-anhydro-7,8,10-tri-O-benzyl-1,4,6-trideoxy-D-manno-deco-2,3-diulose

Guidance literature:: (1R)-1,5-anhydro-3,4,6-tri-O-benzyl-1-(2-butynyl)-2-deoxy-D-arabino-hexitol; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo702663w