n-butyl benzyl trithiocarbonate

Base Information

Chemical Name:n-butyl benzyl trithiocarbonate
CAS No.:82843-63-8
Molecular Formula:C₁₂H₁₆S₃
Molecular Weight:256.457
Hs Code.:

Synonyms:n-butyl benzyl trithiocarbonate

Suppliers and Price of n-butyl benzyl trithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-butyl benzyl trithiocarbonate

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Technology Process of n-butyl benzyl trithiocarbonate

There total 5 articles about n-butyl benzyl trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-15-0,12122-00-8
carbon disulfide

: 109-79-5
n-butanethiol

: 100-39-0
benzyl bromide

: 82843-63-8
n-butyl benzyl trithiocarbonate

Guidance literature:: n-butanethiol; With triethylamine; In chloroform; at 20 ℃; for 0.5h; Enzymatic reaction;

carbon disulfide; In chloroform; at 20 ℃;

benzyl bromide; In chloroform; at 20 ℃;
DOI:10.1021/jacs.8b08386

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 109-79-5
n-butanethiol

: 100-44-7
benzyl chloride

: 82843-63-8
n-butyl benzyl trithiocarbonate

Guidance literature:: With potassium hydroxide; Aliquat 336; Yield given. Multistep reaction; 1.) room temp., 15 min., 2.) 70 deg C, 15 min.;
DOI:10.1055/s-1986-31819

Reference yield:

: 100-53-8
phenylmethanethiol

: 82843-63-8
n-butyl benzyl trithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / ZnCl₂ / 24 h / Ambient temperature

2: 1.) butyllithium / 1.) THF, -10 deg C to -5 deg C, 30 min, 2.) THF, from -10 deg C to RT, 5 h

With n-butyllithium; zinc(II) chloride;
DOI:10.1246/bcsj.55.1977