C₂₉H₄₅N₅O₆

Base Information

Chemical Name:C₂₉H₄₅N₅O₆
CAS No.:1255213-18-3
Molecular Formula:C₂₉H₄₅N₅O₆
Molecular Weight:559.706
Hs Code.:

C<sub>29</sub>H<sub>45</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₂₉H₄₅N₅O₆

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Chemical Property of C₂₉H₄₅N₅O₆

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Technology Process of C₂₉H₄₅N₅O₆

There total 13 articles about C₂₉H₄₅N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1255213-10-5
C₂₉H₄₅N₅O₆

: 1255213-18-3
C₂₉H₄₅N₅O₆

Guidance literature:: With solid-phase supported CuPF₆; In toluene; at 55 ℃; for 16h;
DOI:10.1021/ja105119r

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1255213-18-3
C₂₉H₄₅N₅O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Reflux; Inert atmosphere

1.2: 3 h / Reflux

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 3 h / -78 - 20 °C

7.1: solid-phase supported CuPF₆ / toluene / 16 h / 55 °C

With dimethylsulfide borane complex; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hexamethyldisilazane; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ja105119r

Reference yield:

: 57561-39-4
methyl(2-hydroxyethyl)carbamic acid tert-butyl ester

: 1255213-18-3
C₂₉H₄₅N₅O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 3 h / -70 °C

2.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / dichloromethane / 2.75 h / -78 - -65 °C / Inert atmosphere

2.2: 3.25 h / -78 - -67 °C

3.1: water; dihydrogen peroxide; sodium hydroxide / methanol; tert-butyl alcohol / 0 - 20 °C

3.2: pH 4

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere

7.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 °C

9.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 3 h / -78 - 20 °C

10.1: solid-phase supported CuPF₆ / toluene / 16 h / 55 °C

With 2,6-dimethylpyridine; oxalyl dichloride; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; dihydrogen peroxide; sodium hexamethyldisilazane; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/ja105119r