1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

Base Information

Chemical Name:1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol
CAS No.:949089-43-4
Molecular Formula:C₂₄H₃₉F₃O₂Si
Molecular Weight:444.653
Hs Code.:

Synonyms:1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

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Chemical Property of 1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

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Technology Process of 1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

There total 1 articles about 1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.3%

: 949089-42-3
(2-bromo-5-(trifluoromethyl)benzyloxy)triisopropylsilane

: 502-42-1
cycloheptanone

: 949089-43-4
1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

Guidance literature:: (2-bromo-5-(trifluoromethyl)benzyloxy)triisopropylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

cycloheptanone; In tetrahydrofuran; hexane; at -78 ℃; for 2.1h;

With ammonium chloride; In tetrahydrofuran; hexane; water;

Reference yield: 95.2%

: 949089-43-4
1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol

: 74-88-4
methyl iodide

: 949089-44-5
(2-(1-methoxycycloheptyl)-5-(trifluoromethyl)benzyloxy)triisopropylsilane

Guidance literature:: 1-(4-(trifluoromethyl)-2-((triisopropylsilyloxy)methyl)phenyl)cycloheptanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h;

methyl iodide; In tetrahydrofuran; for 16h;

methyl iodide; With sodium hydride; more than 3 stages;