Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

Base Information

• Chemical Name: Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat
• CAS No.: 95580-44-2
• Molecular Formula: C₂₀H₂₇NO₈
• Molecular Weight: 409.436
• Mol file: 95580-44-2.mol

Synonyms:Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

Chemical Property of Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat

There total 3 articles about Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Ethyl-6-amino-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-5-O,6-N-methylidyn-L-glycero-α-D-glucoheptofuranuronat (95672-73-4) → Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat (95580-44-2)

Guidance literature:

With water; at 60 ℃; for 12h;

DOI:10.1002/jlac.198519850113

Reference yield:

Ethyl isocyanoacetate (2999-46-4) → Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat (95580-44-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaCN / 1.) ethanol, 15 min; 2.) ethanol, 10 min

2: 98 percent / H₂O / 12 h / 60 °C

With sodium cyanide; water;

DOI:10.1002/jlac.198519850113

Reference yield:

3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose (23558-05-6) → Ethyl-3-O-benzyl-6-desoxy-6-formamido-1,2-O-isopropyliden-L-glycero-α-D-gluco-heptofuranuronat (95580-44-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaCN / 1.) ethanol, 15 min; 2.) ethanol, 10 min

2: 98 percent / H₂O / 12 h / 60 °C

With sodium cyanide; water;

DOI:10.1002/jlac.198519850113

upstream raw materials:

Ethyl-6-amino-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-5-O,6-N-methylidyn-L-glycero-α-D-glucoheptofuranuronat

Ethyl isocyanoacetate

3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose