((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

Base Information

Chemical Name:((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate
CAS No.:1432755-23-1
Molecular Formula:C₂₃H₂₇NO₂
Molecular Weight:349.473
Hs Code.:

Synonyms:((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

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Chemical Property of ((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

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Technology Process of ((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

There total 6 articles about ((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 591-80-0
pent-4-enoic acid

: 1432755-04-8
((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methanol

: 1432755-23-1
((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene; at 20 ℃; for 3h;
DOI:10.1039/c3cc41785a

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 1432755-23-1
((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine / ethanol / 60 h / 20 °C

2: sodium tetrahydroborate / ethanol / 0 °C

3: dicyclohexyl-carbodiimide; dmap / toluene / 3 h / 20 °C

With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In ethanol; toluene;
DOI:10.1039/c3cc41785a

Reference yield:

: 284049-37-2
1-allyl-2-vinyl-1H-pyrrole

: 1432755-23-1
((1R,2R,4S)-2-(1-allyl-1H-pyrrol-2-yl)-4-phenylcyclobutyl)methyl pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine / ethanol / 60 h / 20 °C

2: sodium tetrahydroborate / ethanol / 0 °C

3: dicyclohexyl-carbodiimide; dmap / toluene / 3 h / 20 °C

With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In ethanol; toluene;
DOI:10.1039/c3cc41785a