2-Ethenyl-1-prop-2-enylpyrrole

Base Information

Chemical Name:2-Ethenyl-1-prop-2-enylpyrrole
CAS No.:284049-37-2
Molecular Formula:C9H11 N
Molecular Weight:133.193
Hs Code.:
DSSTox Substance ID:DTXSID601283786
Nikkaji Number:J1.372.741D
Mol file:284049-37-2.mol

Synonyms:284049-37-2;SCHEMBL2813908;DTXSID601283786;2-Ethenyl-1-(2-propen-1-yl)-1H-pyrrole

Suppliers and Price of 2-Ethenyl-1-prop-2-enylpyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2-Ethenyl-1-prop-2-enylpyrrole

Chemical Property:

PSA：4.93000
LogP:2.31710
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:133.089149355
Heavy Atom Count:10
Complexity:129

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCN1C=CC=C1C=C

Technology Process of 2-Ethenyl-1-prop-2-enylpyrrole

There total 2 articles about 2-Ethenyl-1-prop-2-enylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 101001-68-7
1-allyl-1H-pyrrole-2-carbaldehyde

: 284049-37-2
1-allyl-2-vinyl-1H-pyrrole

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;

1-allyl-1H-pyrrole-2-carbaldehyde; In tetrahydrofuran; at 0 - 50 ℃; Inert atmosphere;
DOI:10.1039/c3cc41785a

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 284049-37-2
1-allyl-2-vinyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 20 °C

2: 1.47 g / Kt-OBu / diethyl ether / Heating

With potassium tert-butylate; potassium carbonate; In diethyl ether; acetonitrile; 1: allylation / 2: Wittig reaction;
DOI:10.1021/jo0000527

Reference yield:

: 4549-82-0,93614-78-9
(E)-2-methylcinnamaldehyde

: 284049-37-2
1-allyl-2-vinyl-1H-pyrrole

: C₁₉H₂₁NO

Guidance literature:: With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; In ethanol; at 20 ℃; for 72h; enantioselective reaction;
DOI:10.1039/c3cc41785a