4-Iodo-2-nitroanisole

Base Information

Chemical Name:4-Iodo-2-nitroanisole
CAS No.:52692-09-8
Molecular Formula:C7H6INO3
Molecular Weight:279.034
Hs Code.:2909309090
European Community (EC) Number:678-890-0
DSSTox Substance ID:DTXSID20482369
Nikkaji Number:J465.155C
Wikidata:Q72484151
Mol file:52692-09-8.mol

Synonyms:4-Iodo-2-nitroanisole;52692-09-8;4-iodo-1-methoxy-2-nitrobenzene;2-Nitro-4-iodoanisole;Benzene, 4-iodo-1-methoxy-2-nitro-;4-iodo-1-methoxy-2-nitro-benzene;4-methoxy-3-nitroiodobenzene;SCHEMBL1026500;DTXSID20482369;WULXGCDMVLQZBT-UHFFFAOYSA-N;2,6-DIMETHOXYBENZYLALCOHOL;MFCD08060933;4-iodanyl-1-methoxy-2-nitro-benzene;AKOS015890342;CS-W012289;DS-4063;AC-22952;AM20040632;FT-0640095;A829205

Suppliers and Price of 4-Iodo-2-nitroanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Iodo-2-nitroanisole
100mg
$ 60.00

TRC
4-Iodo-2-nitroanisole
50mg
$ 45.00

SynQuest Laboratories
4-Iodo-2-nitroanisole
5 g
$ 458.00

SynQuest Laboratories
4-Iodo-2-nitroanisole
1 g
$ 116.00

Matrix Scientific
4-Iodo-1-methoxy-2-nitrobenzene 95+%
5g
$ 216.00

Matrix Scientific
4-Iodo-1-methoxy-2-nitrobenzene 95+%
1g
$ 72.00

Crysdot
4-Iodo-1-methoxy-2-nitrobenzene 97%
5g
$ 131.00

American Custom Chemicals Corporation
4-IODO-2-NITROANISOLE 95.00%
1G
$ 637.91

American Custom Chemicals Corporation
4-IODO-2-NITROANISOLE 95.00%
5G
$ 914.41

Alichem
4-Iodo-2-nitroanisole
1g
$ 1445.30

Total 31 raw suppliers

Chemical Property of 4-Iodo-2-nitroanisole

Chemical Property:

Vapor Pressure:0.000313mmHg at 25°C
Melting Point:96-98°C
Refractive Index:1.629
Boiling Point:330.8 °C at 760 mmHg
Flash Point:153.9 °C
PSA：55.05000
Density:1.893g/cm³
LogP:2.73120
Sensitive.:Light Sensitive
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:278.93924
Heavy Atom Count:12
Complexity:171

Purity/Quality:

99%, ^*data from raw suppliers

4-Iodo-2-nitroanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 23/24/25
Safety Statements: 36/37-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)I)[N+](=O)[O-]

Technology Process of 4-Iodo-2-nitroanisole

There total 14 articles about 4-Iodo-2-nitroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 91-23-6
2-Nitroanisole

: 52692-09-8
4-iodo-2-nitroanisole

Guidance literature:: With N-iodo-succinimide; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); In 1,2-dichloro-ethane; toluene; at 85 ℃; for 14h; regioselective reaction;
DOI:10.1055/s-0033-1340321

Reference yield: 88.0%

: 696-62-8
para-iodoanisole

: 52692-09-8
4-iodo-2-nitroanisole

Guidance literature:: With N-Bromosuccinimide; silver nitrate; In acetonitrile; for 5h; Reflux;
DOI:10.1016/j.tetlet.2012.06.126

Reference yield: 69.0%

: 4920-80-3
3-methoxy-2-nitrobenzoic acid

: 52692-09-8
4-iodo-2-nitroanisole

Guidance literature:: With copper(I) oxide; potassium phosphate; bismuth (III) nitrate pentahydrate; palladium(II) trifluoroacetate; oxygen; sodium iodide; In dimethyl sulfoxide; at 170 ℃; for 10h; regioselective reaction; Schlenk technique; Green chemistry;
DOI:10.1021/acs.orglett.9b00460