Technology Process of C29H33NO10P2
There total 16 articles about C29H33NO10P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; trichlorophosphate;
at -15 - 20 ℃;
for 4.33h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 0.75 h / -10 - 0 °C
2: piperidine / toluene / 24 h / Reflux
3: tetrahydrofuran / 6 h / 0 - 20 °C
4: acetic acid; water / 2 h / 90 °C
5: pyridine; trichlorophosphate / 4.33 h / -15 - 20 °C / Inert atmosphere
With
piperidine; pyridine; water; toluene-4-sulfonic acid; acetic acid; trichlorophosphate;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: boron trifluoride diethyl etherate / toluene / 1.5 h / 100 - 108 °C / Inert atmosphere
2: toluene-4-sulfonic acid / 0.75 h / -10 - 0 °C
3: piperidine / toluene / 24 h / Reflux
4: tetrahydrofuran / 6 h / 0 - 20 °C
5: acetic acid; water / 2 h / 90 °C
6: pyridine; trichlorophosphate / 4.33 h / -15 - 20 °C / Inert atmosphere
With
piperidine; pyridine; boron trifluoride diethyl etherate; water; toluene-4-sulfonic acid; acetic acid; trichlorophosphate;
In
tetrahydrofuran; toluene;