(2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol

Base Information

• Chemical Name: (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol
• CAS No.: 852395-56-3
• Molecular Formula: C₇₁H₇₆O₁₃
• Molecular Weight: 1137.38

Synonyms:(2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol

Chemical Property of (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol

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Technology Process of (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol

There total 1 articles about (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(2R*)-2-O-benzoyl-1,3-bis-O-(2,3,4,6-tetra-O-benzyl-D-mannopyranosyl)glycerol → (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol (852395-56-3) + 1,3-bis-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)glycerol (852395-55-2)

Guidance literature:

(2R*)-2-O-benzoyl-1,3-bis-O-(2,3,4,6-tetra-O-benzyl-D-mannopyranosyl)glycerol; With sodium methylate; In methanol; at 20 ℃;

With hydrogenchloride; In dichloromethane; water;

DOI:10.1016/j.bmc.2010.11.058

Reference yield: 76.0%

(2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol (852395-56-3) + 1,2-di-O-stearoyl-sn-glycero-3-H-phosphonate triethylammonium salt → 2-O-(1,2-di-O-stearoyl-sn-glycero-3-phosphoryl)-1,3-bis-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)glycerol triethylammonium salt

Guidance literature:

(2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol; 1,2-di-O-stearoyl-sn-glycero-3-H-phosphonate triethylammonium salt; With pyridine; pivaloyl chloride; at 20 ℃; for 1h;

With iodine; In pyridine; water; at 20 ℃; for 0.75h;

Reference yield: 64.0%

benzyl-octadecanyl-N,N-diisopropylphosphoramidite (852395-86-9) + (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol (852395-56-3) → 2-O-(benzyl-octadecyl-phosphoryl)-1,3-bis-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)glycerol

Guidance literature:

benzyl-octadecanyl-N,N-diisopropylphosphoramidite; (2R*)-1-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)-glycerol; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 2h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

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